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Technical Nickel plating small hardware --

Discussion in 'Traditional Hot Rods' started by goodfellow, Oct 22, 2013.

  1. goodfellow
    Joined: Feb 12, 2007
    Posts: 30

    goodfellow
    Member
    from Virginia

    I was asked to post this by a fellow HAMB member. Hope you find it useful -

    Part 1:

    This is a small electroplating setup that I have used successfully over the years. I've scaled this design up to successfully plate larger parts, including a motorcycle fender and automotive gauge housings, and also scaled it way down to plate small machine screws and other hardware. Today I'm going somewhat small, since this plating process is designed to nickel plate larger sized fasteners and brackets for a car restoration.

    Also, when I say that I've done "plating" with these setups, I mean mostly nickel and zinc plating. I've never attempted chrome.

    First I needed a small plastic tub -- pretty cheap enough from Target. A lid is good, since it will allow me to store the plating solution safely when finished. This tub holds about 1 gallon of solution max, but I won't use that much -- maybe 1/2 to 3/4 gal. We'll address the plating solution later.

    [​IMG]

    [​IMG]

    Next, I cut two 6" nickel anodes in half to produce four 3" strips (google "nickel anode" and you'll get plenty of offerings)

    [​IMG]

    The anodes need to be firmly affixed to the exterior walls of the tub. To do that. I drilled some 1/8" holes in each anode and also 1/8" holes into one side of four clothespins. The IMPORTANT part here is that the electrical connections need to be as sound as possible. To that end, I cut 4 pieces of 14ga electrical wire to accept round crimp terminals, and mounted the wire and anode to the clothespins.

    [​IMG]

    [​IMG]

    Next, I needed to build a "bubbler" for this tub. The bubble's job is to keep the solution agitated enough to make the nickel ions propagate evenly and steadily through the solution. You can plate without the bubbler, but the plating will most likely be uneven and spotty. If you want to skip the bubbler, then just use a wooden spoon to keep the plating solution agitated at a slow but constant speed -- but that can get tiring if you want to plate a good quantity of parts.

    The bubbler starts out as 1/4" clear tubing that is hot glued into the bottom of the tub. The best solution is to use a curved wide "S" pattern to get good coverage of the base. I glue both end up the side corners of the tub so that there is plenty of excess tubing for connections and external fittings.

    [​IMG]

    One end is capped with a bolt and a hose clamp, the other is attached to a barbed fitting and a small air pressure regulator. You want the end with the bolt to be removable in order to clear any remaining fluid from the bubbler tube during a complete cleanup. A quick burst of air and the tube will clear. Just don't put the metal end cap bolt in the solution itself -- it will contaminate the plating solution.

    [​IMG]

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    Once the tube is glued in place, I pressurize the tube with 10-15 psi and use a sharp pick to make five holes in the tube -- one in each corner and one in the middle of the tub.

    [​IMG]

    Here is the first stage with all the positive anode leads completed --

    [​IMG]

    Next comes the cathode (negative)****embly. Here I used a piece of 3/8" flexible copper tubing and flattened the ends to again attach 14ga wire on each end with round crimp connectors. Again, I want the best electrical flow possible, so I used two connections instead of one.

    [​IMG]

    [​IMG]

    Once all the positive and negative connections were in place, I terminated each of the negative and positive wire bundles into a larger gauge bus wire so that the electrical load can be easily distributed. This is overkill, but you don't want to take a chance with voltage drop in the plating process. Notice the bundled connections in the lower parts of the pics. These bus connections were soldered and insulated with shrink tubing.

    Finished with the tub!

    [​IMG]

    [​IMG]

    The plating solution for this nickel process is comprised of Nickel Sulfate, Ammonium Chloride and Boric Acid -- I didn't come up with this solution. It was gleaned from the following website -- http://www.substech.com/dokuwiki/doku.php?id=nickel_electroplating

    [​IMG]

    It's the last category called "Hard Nickel Plating" --

    Here are some of the specs for the process -- You can try the process without the boric acid, but in my opinion, the nickel becomes too brittle and will flake off much more readily; not something I want to happen to my frame and carriage hardware.

    Bath composition:
    Nickel sulphate, NiSO46H2O: 24 oz/gal (180 g/l)
    Ammonium chloride, NH4Cl3: 3.3 oz/gal (25 g/l)
    Boric acid, H3BO3: 4 oz/gal (30 g/l)

    Operating conditions:
    Temperature: 110-140°F (43-60°C)
    Cathode current density: 25-50 A/ft² (2.5-5 A/dm²) PH: 5.6-5.9

    Also, I've noticed that given the size of the container and parts, you can get great results with just a plain battery charger; so DON"T****ume that maximum voltage and amperage will yield a good plating job. In fact, just the opposite is true -- in a small container, low voltage and low amperage yields the best results. So a small battery charger will suffice.

    For big plating jobs that have a large surface area, you need more current and better control of voltage. A variable power supply like this Lambda has enough amperage and voltage to plate large pieces.

    [​IMG]

    [​IMG]

    However, for small hardware and brackets, a small battery charger set at 2 amps and pushing 6 volts is sufficient for the job!
     
    Last edited: Oct 22, 2013
  2. goodfellow
    Joined: Feb 12, 2007
    Posts: 30

    goodfellow
    Member
    from Virginia

    Part 2:

    Ok, now it's time to do the prep work. Like everything with cars, it's the prep that takes the most time; the plating itself takes less than an hour. Here are the subframe bolts from my car. They show some flash rust and shadow corrosion.

    [​IMG]

    First cleaning is done on the wire wheel. The rust and scale is wheeled off to reveal a nice clean finish. Every nut, bolt and washer gets wheeled -- Here are all the cleaned pieces. I used a protective mask and latex gloves to wheel this hardware since it was originally cadmium plated --

    [​IMG]

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    Next the remaining plating and micro-rust spots need to be removed by submerging the hardware in distilled vinegar. You can see that although these pieces were cleaned with the wire wheel, the vinegar reacts pretty aggressively with the remaining plating and rust.

    NOTE: The fumes from this dissolving plating are dangerous, and they are quite strong -- you need ventilation; so I just set this cup outside in the fresh air and waited for two hours for the bubbles to subside.

    [​IMG]

    Once the vinegar does its job, I rinsed the hardware in fresh water and what's left is a black loose oxide on the surface of the hardware.

    [​IMG]

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    Now it's back to the bench grinder and another wheeling session to get rid of the oxide coating. Now look at the comparison between the oxide and the wheeled hardware. What's left is pure virgin steel!!!

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    When all the hardware is wheeled, each piece is rubbed down with rubbing alcohol to remove the oil from my hands and fingers. I wear latex gloves for this process. If there's oil on the steel then it won't plate evenly.

    Now let's set up the plating solution -- first a cheap kitchen scale, copper wire for hanging parts on the cathode rail (negative side), and distilled water. This is important. If you live in areas with mineral rich water (i.e. iron or high sulphur), then the plating may not work very well. To be on the safe side I always use distilled water.

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    I used a gallon of distilled water heated to 150F and weighed out the following proportions

    Nickel Sulphate -- 24oz
    Ammonium Chloride --- 3.3oz
    Boric Acid --- 4oz

    Note -- wear gloves and a good dust mask when handling the dry ingredients --

    [​IMG]

    [​IMG]

    Everything was stirred slowly to make sure the ingredients dissolved properly, and then the rubbing alcohol cleaned parts were set up in ****embly line fashion.

    [​IMG]

    Now all the electrical connections are made, and the bubbler is started --

    [​IMG]

    Plating nuts/bolts for too long will change the dimensions -- so you need to be aware that leaving the bolts/nuts in the solution for too long may make them useless, and you'll need to chase threads -- that leaves the bolts/nuts open for corrosion again.

    Here I pulled two bolts after 30 seconds and tested some nuts -- they still fit well, so I decided to put them back in the bath and give each part one minute in the solution

    [​IMG]

    IMPORTANT: When you pull the newly plated part from the plating solution, don't just lay it on a towel. It needs to be immediately rinsed in fresh water to get the solution off the part. Failure to do this will result in a tarnished looking part within minutes of the plating process.

    The results are pretty amazing -- nice nickel finish! Beautiful !!!

    [​IMG]

    All the parts nicely hung up on the negatively charged copper pipe and happily bubbling away -- this took about an hour to do. Prep time was about three hours -- LOL

    [​IMG]

    A bench filled with nicely plated hardware ---

    [​IMG]

    I can polish these pieces to a very bright Chrome-like finish, but I prefer a traditional look that reflects the OEM look of the hardware.
     
    FrozenMerc and dos zetas like this.
  3. goodfellow
    Joined: Feb 12, 2007
    Posts: 30

    goodfellow
    Member
    from Virginia

    Beautiful!! -- the prep work is the key. Well done --
     
  4. ago
    Joined: Oct 12, 2005
    Posts: 2,198

    ago
    Member
    from pgh. pa.

    Amazing what you can learn from this forum, Thanks.


    Ago
     
  5. bobby_Socks
    Joined: Apr 12, 2006
    Posts: 938

    bobby_Socks
    Member
    from ǑǃƕǑ

    Great Tech article. Wondering if this works only on steel or if it will also work on Stainless Steel ? Will it work on Aluminum without a Copper coat first being applied ? thanks again
     
  6. sidevalve8ba
    Joined: Jun 16, 2009
    Posts: 2,597

    sidevalve8ba
    ALLIANCE MEMBER

  7. goodfellow
    Joined: Feb 12, 2007
    Posts: 30

    goodfellow
    Member
    from Virginia

    Should work on both, but by adding the copper as a sublayer, you get a much deeper bright nickel finish that can be polished to look like chrome
     
  8. 56don
    Joined: Dec 11, 2005
    Posts: 10,329

    56don
    Member

    One of the most simply laid out tech pieces I have read on here. Easy to follow. Thanks.
     
  9. chickenshift
    Joined: Feb 14, 2010
    Posts: 363

    chickenshift
    Member

    very cool! I cant wait to try this
     
  10. Tim_with_a_T
    Joined: Apr 30, 2011
    Posts: 1,738

    Tim_with_a_T
    Member

    Excellent post. Not to be the safety police, but if I were to try this, I'd be wearing a face shield, long rubber gloves at least as thick as dishwashing gloves, and an acid apron. I would also have a secondary containment for the plating solution in case of a spill and fresh water close by.
    Now for the stupid questions. How do you dispose of the solution when you're finished plating? Is it re-usable? Is it safe to dilute and dump down the drain, or is that a big no no? Again, very informative post. Thank you.
     
  11. mattrod68
    Joined: Jan 22, 2007
    Posts: 517

    mattrod68
    Member

    your my hero, very cool. im now looking for things to plate.
     
  12. NoSurf
    Joined: Jul 26, 2002
    Posts: 4,822

    NoSurf
    Member

    Nice Job.

    Thank you for taking the time to take the pics and post up the explanation.
     
  13. RainierHooker
    Joined: Dec 20, 2011
    Posts: 2,031

    RainierHooker
    Member
    from Tacoma, WA

    Wow, thanks for posting this.

    I'll definately be using this soon, on the car, and my old nickel-plated bathroom hardware!
     
  14. cederholm
    Joined: May 6, 2006
    Posts: 1,754

    cederholm
    Member

    What a great write-up, THNX!!

    Can you do pot metal this way? I'm thinking hood ornaments.

    ~ Carl
     
  15. sidevalve8ba
    Joined: Jun 16, 2009
    Posts: 2,597

    sidevalve8ba
    ALLIANCE MEMBER

    Where would you buy the chemicals needed to do this plating?
     
  16. Bugguts
    Joined: Aug 13, 2011
    Posts: 990

    Bugguts
    Member

    Great tech!
    Since all my questions have been asked, I'm subscribed and looking forward to the answers.
     
  17. need louvers ?
    Joined: Nov 20, 2008
    Posts: 12,901

    need louvers ?
    Member


    Neat! Very well written tech, but I have to second the question. Is this all stuff that is commonly available without being put on some sort of government "watch list" type non-sense?
     
  18. goodfellow
    Joined: Feb 12, 2007
    Posts: 30

    goodfellow
    Member
    from Virginia

    The chemicals were purchased through Amazon from a commercial supplier that sells through that site.

    http://www.amazon.com/gp/aag/main?i...D=ATVPDKIKX0DER&orderID=&seller=A2QI1LLWJGHHE

    I just checked the site, and it seems that they are sold out of the Nickel Sulfate -- hmmm -- there must be run on that stuff. Wonder why? --LOL
     
    Last edited: Oct 22, 2013
  19. noboD
    Joined: Jan 29, 2004
    Posts: 8,960

    noboD
    Member

    Thank you!!
     
  20. 55Hydramatic
    Joined: Apr 24, 2011
    Posts: 458

    55Hydramatic
    Member

    Awesome! Going to try it! Thanks for the write up!
     
  21. go-twichy
    Joined: Jul 22, 2010
    Posts: 1,648

    go-twichy
    BANNED

  22. I am having trouble getting a piece of nickel to use, the closest I can get is nickel wire. Has anyone used this with success? Or is there something which has a lump of nickel in it which can be scrounged?
     
  23. goodfellow
    Joined: Feb 12, 2007
    Posts: 30

    goodfellow
    Member
    from Virginia

  24. gotit
    Joined: Aug 27, 2009
    Posts: 357

    gotit
    Member

    Put it right back in the earth. Isn't that where it came from?
     
  25. goodfellow
    Joined: Feb 12, 2007
    Posts: 30

    goodfellow
    Member
    from Virginia

    You can filter the solution through a paper towel and then reuse it, but don't dump it. It is toxic, so wear gloves and take appropriate measures to protect yourself. You can dispose of it through your local community landfill if they have a separate section for diposing of volatile fluids, paints, corrosives etc..
     
  26. 36cab
    Joined: Dec 2, 2008
    Posts: 959

    36cab
    ALLIANCE MEMBER

    [​IMG]

    Man does that photo of the parts hanging in the nickel bath bring back memories of my old plating days! There is nothing better than a green bubbling nickel bath. I was told our tanks were the biggest west of the Mississippi River. They were big enough that we plated a few complete small car frames like Fad Ts and Model As.
     
  27. seb fontana
    Joined: Sep 1, 2005
    Posts: 9,178

    seb fontana
    Member
    from ct

    Ah, the bubbler! Forgot about that when I zinc plated a shifter lever at home and did the stir with a stick routine, yep tiring..How big a of a part would you attemp to plate in place of the bolts/nuts? Nice build !!!!
     

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